Above: (first row) 8“ Entegris wafer carrier, 6” SEP wafer carrier, (second row) blue tape diced wafer w/ top film cover, simple plastic case for metal mask, red plastic case for mask, wafer held in simple plastic case, green test tube rack for dies in micro-centrifuge tubes, (third row) Fluoroware mask holder, Fluoroware 4“ wafer holder, wafers in plastic case, vacuum sealed wafer.

This page covers ways to store samples, with a focus on after decapping.

General notes

Residual acids will cause corrosion, so make sure to wash well. I've generally not had issues with dies scratching each other, but anything valuable is stored individually.

Die

Centrifuge

mcmaster preferred solution for general storage

Size: Most dies are small, say less than 4 mm. Micro-centrifuging tubes work well and can be put into racks or small cabinets. Typically I put dies in 1.5 mL tubes but use 5 mL tubes for larger samples. Over that (uncommon) I'll typically used more specialized storage such as pillowstat boxes or sticky films (see later sections). Note that 0.5 mL look the same as the 1.5 mL tubes but have less volume inside, don't buy them.

Label: I typically wrap a Brother label around them. Prefer specifically the Brother PT-2030 (over say the PT-2730). In margin: short mode it prints the label justified to the right with a leader on the other side. This makes it easy to wrap around tubes and still get nice centered text. Messy handwriting aside, permanent marker labels can rub or be washed off with acetone.

Image Vendor Model Size Material, body Material, cap O-ring Skirt? Rounded? Description Notes
vwr_1.5ml_bag_label.jpg VWR 20170-213 1.5 mL PP? Pink Y Y N SCREW CAP TOP WITH SKIRT Retail: looks to be about $144/1000 (includes cap)
eBay 2012?: paid about 30 for a mostly full bag
Has o-ring
AGILENT TECHNOLOGIES 5188-5251 1.5 mL Y N N MICRO TUBE, SCREW TOP 2015?: liberated from noisebridge
Retail: $37/100 (includes cap)
Not skirted. I tend to prefer skirted
? ? 1.5 mL PP N/A N N N Primary tube in use
Security lock: lid snaps on very securely
eBay 2014: 500 / bag, $15 shipped
Savillex 200-915-50
600-011-83
1.5 mL PFA PFA N N N Link
2018 new: $8.30 *each*
I was getting these for WFNA work, but found that polypropylene is actually fine, despite compatibility chart notes
mc01050.jpg Lion International MC01050 5 mL PP N/A N N Y Used for medium dies
JIUWU 5 mL “Plastic” N/A N DIY Crafts India 221
corning_430791.jpg Corning CentriStar 15 mL PP Orange N N N Use for storing bulk dies, like from RAM
eBay 2014: $14 shipped for 25
Biologix 50 mL PP PVC? N N N eBay 2010: $5 / 50
Use as temp storage when working (individual dies, decapped DIPs)
Use for measuring chemicals
Image Vendor Model Tube size(s) Tube count Material Description Notes
Custom? Custom? 50 mL 25 Polypropylene?
White
mcmaster: really like these
Heavy duty
eBay 2014: 6 for $90 shipped
Difficult to knock over
? 10/15 mL: 30
50 mL: 20
Polypropylene
Orange
Snaps together
2013: $10 shipped
Light, but usually gets the job done
PUL FACTORY PUL13007 5 mL 32 Polypropylene
White + blue
Link
Putting the rack in the lid to put into ultrasound
Karter Scientific? 235I2? 0.5 mL
1.5 mL
Polypropylene?
Multicolor
mcmaster: really like these
eBay? Can't find purchase notes
PAT NO D-359,126

Membrane box

https://www.youtube.com/watch?v=9CYetdKGegU

These containers suspend a sample in the center between one or more thin films. Sometimes, although not always, the films are slightly sticky to help keep the sample in place. I am fond of these for large dies, but I haven't invested in getting a lot of them.

Gel

Gel boxes are common in the electronics industry for storing many dies for repackaging. However, I don't like them because 1) I've had issues with large dies sticking and breaking when removing 2) you need to index the dies externally to indicate what they are. However, I'd probably use them if I needed to storage a large number of identical dies.

ESD box

mcmaster: for decapped large packages (ex: PGA) I use CCI Pillowstat containers (example)

Wafer

Wafers should be stored in standard wafer cassettes. Polypropylene units can be found fairly inexpensive on eBay (ie don't go nuts and buy a PFA cassette since it may cost $200).

Cassette / carrier

Most common form for holding bulk wafers for transport. Entegris/Fluoroware seems to be a popular brand.

Above: 6” simple polypropylene Entegris ULTRAPAK 150mm carrier with wafers. Three pieces: box top, box bottom, and wafer carrier. Also if you look closely you'll notice that I have more than one wafer per slot…don't do that for wafers you care about. I have extra blank wafers that I was either going to throw away or stack up.

Above: Shin-Etsu Polymer Co., Ltd. MW200-N 200mm with wafers, a more complex device for holding 8“ wafers. Same basic parts as previous but wafers are now spring loaded instead of held in place by the box itself and there is a gasket ring to keep it sealed better. Looks like a few different materials were used as well instead of being uniform PP.

Fabs use special robotic types depending on the technology. 6” typically use Smif interface while 8“ uses FOUP.

Boat

Used for temporary storage. Fused silica boats are used to anneal wafers.

Twist lock

Most common form for holding small quantities of wafers for transport. Above: Fluroware H22-30 4” single wafer twist lock carrier.

Blue tape

Diced wafers are usually on blue tape. Thin plastic films should stick easily to seal it up.

Vacuum pack

I've seen some wafers vacuum packed but presumably only when used for display. A good example are the “Intel: Journey inside the computer” kit wafers.

Mask

Above: Fluoroware H92-500IPW mask holder with mask. Note the nub in each corner so that only the side of the mask is touched.

Foams

This section was added to try to learn why some black conductive foams degrade into powder and others degrade into a (mildly corrosive?) sticky mess

Terms [Foam vs]:

  • Conductive: surface resistance < 1 x 10 5 ohms/square
  • Dissipative: 1 x 10 5 ohms/square < surface resistance < 1 x10 11 ohms/square
  • Insulative: surface resistance > 1 x 10 12 ohms/square
  • Anti-static: inhibits triboelectric charging, “the buildup of an electric charge by the rubbing or contact with another material”

Density

Vendors talk about low and high density foams. There doesn't seem to be any agreement whatsoever as to what these mean, even within the same vendors. Look at the kg/m3 ratings I guess if you care about density

Blowing agent

In order to turn a liquid into a foam, you need a way to aerate it. Looks like traditionally this was done with CFCs but looks like it may now typically be done with nitrogen.

Pink foam

Also seen in the form of bags and packing bubbles.

Alternatives are available, but seems to typically contain amines either coated on the surface or injected into the material to make them static dissipative. In either case that means that it forms a sort of oily coat that can degrade over time as well as coat the product. For example, you should never use pink foam for optical assemblies. Over time this builds up (“blooms”) which makes affixing labels to the surface difficult. A sample product has one year shelf life. [Anti-Static Poly Bags]

Seems that EPE (Expanded Polyethylene) is most common material

Types [Foam materials]:

  • EPS (Expanded Polystyrene)
    • “most resistant to moisture absorption”
    • “acceptable for cold storage applications”
    • “resistant to virtually all aqueous media including dilute acids and alkalis, as well as water-soluble alcohols and silicones”
    • “limited resistance to paraffin oil, vegetable oils, diesel fuel, and Vaseline”
  • EPP (Expanded Polypropylene)
    • “excellent energy absorption”
    • “excellent recoverability from repeated shocks and deformations”
    • “retain their high degree of dimensional stability when exposed to temperature extremes”
  • EPE (Expanded Polyethylene)
    • “can withstand repetitive deformations and still maintain its dimensions and cushioning ability”

Blue foam

Like above, but less sensitive to moisture [Why pink]. Unclear if it has any disadvantages (cost, lifetime, etc)

Black foam

From private communication (speculative but may be good lead):

  • Crosslinked type
    • probably lasts longer but it decays into goo
  • Non-crosslinked
    • lasts shorter and decays into powder
  • how long each one lasts depends on manufacturer, amount of ozone/uv exposure, etc

Some foam is firm and is probably the type that decays into powder. Other is squishy and is possibly the type that decays into goo. This is density of the same foam type or a way to tell the crosslinking? In either case unclear what it means

Maybe could UV irradiate foam to simulate aging

References

 
equipment/storage.txt · Last modified: 2018/12/09 19:19 by mcmaster
 
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